Making Damascus Barrels the movie
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Original finish - Restoration
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Black and White Finish
gun
Courtesy
Black and White Finish
Francotte Boxlock
Courtesy Cabelas Gun Library
Black and White Finish
Francotte Boxlock
Courtesy Cabelas Gun Library
Brown and White Finish
Francotte Boxlock
Courtesy Cabelas Gun Library
Brown and White Finish
Francotte Boxlock
Courtesy Cabelas Gun Library
TEXT HERE
Black Finish
WC Scott
Courtesy of  Champlin Firearms
Etched Finish
Suhl
Courtesy of Champlin Firearms


    In  " Le Damas"   Puraye talks about 4 different methods for finishing a set of
    Damascus barrels.  Black & White, Black, Etched, barrels that were bronzed then
    done in  Black & White. If you know of an example of the bronzed with a Black &
    White finish, we would be happy to place any photos you own on our site.    In
    addition, we also know that a common method in England was called Browning.  If
    you are aware of a 6th method please contact us.

    If you want to refinish a set of barrels yourself, you may want to read this thread.
    Double Gun Refinishing FAQ

    You may prefer to have a professional do the job.  We are familiar with the work of
    each professional here and can recommend them.

    Buck Hamlin           Steve Bertram
    Pevely, MO             Boulder, CO
    636-479-4304        303-938-1996

    Dale Edmonds
    Kansas City, MO
    816-444-2040

    Keith Kearcher
    Bend, OR
    541-617-9299

    Dewey Vicknair
    Ephrata, Pennsylvania
    717-733-2145

    What follows are examples of the various finishes.   
TEXT HERE
Brown Finish
Rigby
Courtesy Cabelas Gun Library
Brown and White Finish
gun
Courtesy Cabelas Gun Library
Browned Finish
Rigby
Courtesy
Brown and White Finish
Francotte Boxlock
Courtesy Cabelas Gun Library
OK.  So you want to do the process yourself.  Here is a primer by Dr Oscar Gaddy

Dr. Oscar Gaddy evolved from 15% ferric chloride to 11%, then to 7.5% for some cases (mostly
depending on ambient temp -- less concentrated in warmer climes).

Coating bores to protect is fine but he relied on solid rubber stoppers when dip etching. For boiling,
each bbl tube got one solid stopper and one with one hole at the other end, with a 90 degree bent
stainless tube to vent the bbl interior to air above the water line.

                               
A Rust Blue Primer
                                    by Oscar Gaddy

With regard to polishing, this should all be done by hand and never with a buffing wheel. The finest
that I usually polish is 320 grit. Any finer than this is wasted effort in my opinion as the etching of
the steel surface by the acidic rusting agents creates a matte finish with more surface variation than
is obtained by polishing with the finer grit papers.

After polishing is completed, the barrel surfaces must be completely degreased before rusting. There
are several ways that this can be done including organic solvents and the lime slurry or whiting
method. I prefer to boil the barrels in a mild solution of potassium hydroxide which saponifies and
removes all greases and oils. The important thing is to use a method that works for you.

After degreasing, the barrels must be handled only when wearing gloves--either rubber or cotton
depending upon whether the barrels are wet or dry. The rusting solution is applied to the barrel
surfaces. I use a 1 inch wide foam paint brush for this. The rusting solution should be applied as
uniformly as possible but it is not extremely critical. The barrels should then be allowed to rust from
12 to 24 hours. Some people use humidity controlled chambers, but I just hang them for rusting in
my unheated and un-air conditioned garage. I live in central Illinois and the humidity of the outdoor
air is seldom below 30 to 40 % year round which is quite adequate for rusting. Do not try to rust
indoors as the indoor humidity is usually too low especially in the winter.

After rusting, the barrels are then boiled in water to convert the brown ferric oxide to the black ferro-
ferric oxide. It is always safest to use rainwater or distilled or deionized water if your water supply is
very hard. Water with large amounts of some minerals have been known to convert the brown oxide
to reddish colored carbonates. After boiling, the excess black oxide is then carded off. I use one of
Brownells wire wheels with .005 in steel wires rotating at about 600 rpm. You can also just use steel
wool and it is much easier to do this with the barrels wet under running water if you do it this way.

After carding, the rusting, boiling and carding process is repeated until the desired black finish is
obtained. The exact number of passes depends upon the rusting solution and the humidity during
rusting. Finally, the barrels are placed in a chemically basic solution such as potassium hydroxide or
sodium bicarbonate to neutralize any acids that remain on the barrel surface or in pores in the metal
in order to prevent any after-rusting. The barrels are then oiled and the bores are polished and the
process is complete.
These are the basics of the process. I will be happy to try to answer any questions.


Rust Bluing Formula per Oscar Gaddy Stock Solution; dilute 1:1 … and up to 1:8 for final rustings.
To make 125 ml Stock Solution:

Conc. HNO3 ..... 3.22 ml

Hg2Cl2 (Mercuric chloride -- DEADLY poison) .... 6.25 gms

C2H5OH ..... 3.25 ml

Fe2Cl3 ..... 5 ml

H2O ..... to make 125 ml

===========================================================

Parker Factory Process Adapted by Oscar Gaddy: (DGJ 1997 #2, #3 & 2003 #1)

1. Prep as in Oscar’s original process [next page], Steps 1 – 7

2. “Light” Etch in “mild” Fe2Cl3 solution [I used 15%, it was hard to maintain even results in hi
ambient temps of FL – Oscar later moved down to ~ 10%, some report using 7.5%]

3. Rust and card once daily, for 7 to 10 days, as in Oscar’s original process, but no boiling (wet
card?) [I dry carded with 0.006 wire wheel, need to check speed, 0.005 or .004 better]

4. Only after 7 to 10 passes, plug bores with rubber stoppers (one in each bore with stainless, ¼,”
90 o degree-bent tube for pressure relief), then boil 5 minutes, in solution of 3.5 ltrs water with 60
cc logwood powder + 30 cc FeSO4 . 7 H2O powder (copperas)

5. Rinse well in cold water

6. Soak ~ 5 minutes in solution of ~ 3.5 ltrs water with 15 cc FeSO4 powder (concentration not
critical) – a finger should be able to rub to show light metal with contrast

7. Scrub with CaCO3 powder picked up on wet towel (paper or cloth)

8. Job should look good, but can be improved if desired by rusting and carding 2 or 3 more times; if
that is done repeat final steps 4 thru 7. [Parker factory on notes 2nd following page]

============================================================

The First Process Oscar Gaddy Published:

1. Metal repairs as required: Raise dents & peen upset metal

2. Strike damaged areas

3. Hand polish to 320 (up to 400 grit) finish (but more is wasted effort, matted by rusting)

4. Drill 2nd hole in bottom rib

5. Degrease (boil in mild KOH, 0.1 - 0.2 N)

6. Remove remaining finish with Naval Jelly [or Brownell’s version for max polish]

7. Scrub with Ajax, rinse thoroughly and dry

8. Rubber stopper and rust with 1:1 dilution of rusting formula listed above; apply with 1 inch foam
paintbrush with excess squeezed out; [make & use rib hole plugs next time]

9. Let stand and rust for 24 hours [but check progress, perhaps shorter time]

10. Boil in distilled H2O for several minutes; dry thoroughly

11. Dry card with 6” diameter wire wheel, 600 RPM, wires 0.006” – minimum pressure against
wheel, (consider 0.005” for less aggressive removal or try hand carding next time)

12. Plug with rubber stoppers; immerse in Fe2Cl3 – commercial solution (Radio Shack) diluted
to15% strength with H2O at room temperature for “a few seconds” – dilute even more, to 10%,
7.5% or perhaps even 5% at higher ambient temperatures -- [ I later learned that one, longer etch
only, before bluing, is OK – see Parker factory process – still ambiguous on this]

13. Quickly rinse in H2O and wet card vigorously with grade 0 steel wool until no more finish can be
removed – if not diluting to or below 10% consider dipping into a PVC pipe water tank rinse [rather
than hose down] to even out etch time breech to muzzle

14. Repeat steps above as indicated, 10 to 15 times, diluting rusting solution after 2 to 3 passes –
typically finishing up with 1:8 dilution for the final rustings – perhaps even lower

15. Immerse in dilute KOH (0.1 - 0.2N) for ~ 1 hour [I repeatedly injected KOH solution into inter-
barrel region and sloshed it around], then …

16. Rinse thoroughly, then …

17. Dry, oil, RIG or wax thoroughly, and …

18. Polish bores, muzzle, lump and breech faces

============================================================

Parker Factory Process (Unmodified, Verbatim from Parker notes – Oscar, 2003)

1. Clean with brush, heat “on steam pipes” until “fairly hot”

2. Wash with H2SO4, diluted 1:2, for 4 or 5 minutes to bring out the figure

3. Wash with water to kill the acid

4. Clean with pumice and water

5. Apply 1st rusting acid: ½ oz HCl + ½ oz CuSO4 in 1 qt water

6. Apply 2nd rusting acid while first is still wet; formula varied for weather:

Dry weather: ½ oz HCl + ½ oz HgCl + ¼ oz Fe2Cl3 in 1 qt water

Damp weather: ¼ oz HCl + ½ oz HgCl in 1 qt water

7. Place in steam dry[er?] for ~ 5 minutes

8. Put over to the side of the room after drying [to rust?]

9. Turn off “wet steam” after rusted and turn on “dry steam” to avoid too much rust

10. Let stand over night

11. Card with wire brush

12. When cold [implies prior step used power] repeat rusting exactly as before, 4 to 6 times

13. Cook in logwood bath 4 to 5 minutes; bath = 2 qts logwood [probably chips] + 4 to 6 ozs
copperas 1.5 ozs CuSO4 in “tank” of water

14. Cool off and place in copperas bath; bath = ½ oz copperas in “tank” of water until finger can rub
off black coating to show white, usually ~ 5 minutes

15. “Wash [implies rub] with whiting [CaSO4 fine powder] until figure shows even”

16. Wash under running water

17. Put into tank of hot water, wash well

18. Dry in sawdust

19. Rust again in two acids as before (Steps 5 & 6)

20. Cook in steam room [one time]

21. Cook in logwood + copperas bath 1 to 3 minutes

22. Put into copperas bath, finish as before
 www.damascus-barrels.com
Belgian Brown and White Finish
unmounted barrels
produced in 1905

Courtesy of Mr Daryl Hallquist